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  • 郭力城,赵湘培,滕红丽.薄层色谱法评价不同产地黄根的品质[J].广西科学院学报,2015,31(4):305-307.    [点击复制]
  • GUO Li-cheng,ZHAO Xiang-pei,TENG Hong-li.Identification of Prismatomeris connate Y.Z.Ruan from Different Origin by TLC[J].Journal of Guangxi Academy of Sciences,2015,31(4):305-307.   [点击复制]
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薄层色谱法评价不同产地黄根的品质
郭力城, 赵湘培, 滕红丽
0
(广西壮族自治区民族医药研究院/广西壮医医院, 广西南宁 530001)
摘要:
[目的]建立评价黄根(Prismatomeris connate Y.Z.Ruan)品质的薄层色谱分析方法。[方法]以有效成分甲基异茜草素为指标,以甲苯-乙酸乙酯-甲醇-甲酸(3:1:0.2:0.1)为展开剂,建立黄根的专属性薄层色谱,并评价10个不同产地黄根的品质。[结果]不同产地黄根药材与对照色谱在相应位置上,显示出相同颜色的斑点,且斑点清晰,比移值(Rf)为0.76。[结论]薄层色谱法能够有效对黄根进行鉴别,且该方法简便、准确,具有较好的适应性。
关键词:  黄根  甲基异茜草素  薄层色谱
DOI:
投稿时间:2015-04-10
基金项目:国家科技支撑计划项目(2012BAI27B06-1,2013BAI11B06-6),广西重大专项计划项目(桂科重14124002-14)和南宁市科技攻关与新产品试制项目(20133158,20133163)资助。
Identification of Prismatomeris connate Y.Z.Ruan from Different Origin by TLC
GUO Li-cheng, ZHAO Xiang-pei, TENG Hong-li
(Guangxi Institute of Minority Medicine/Traditional Zhuang Hospital of Guangxi, Nanning, Guangxi, 530001, China)
Abstract:
[Objective] To establish a TLC method for the identification of Prismatomeris connate Y.Z.Ruan.[Methods] Rubiadin was indicators,methylbenzene-ethyl acetate-methanol-formic acid (3:1:0.2:0.1) was developing agent.[Results] The same color spots were shown in the corresponding position of the Prismatomeris connate Y.Z.Ruan from different origin. The spots were clear and the Rf index was 0.76.[Conclusion] The TLC method is effective for the identification of the Prismatomeris connate Y.Z.Ruan.The method is simple and reliable.
Key words:  Prismatomeris connate Y.Z.Ruan  rubiadin  TLC

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