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刘布鸣,马彦,冯可荣,黄艳,王廷伟,林霄,莫建光.制备高效液相色谱分离纯化系统的研制与开发[J].广西科学院学报,2010,26(3):354-356. [点击复制]
- LIU Bu-ming,MA Yan,FENG Ke-rong,HUANG Yan,WANG Ting-wei,LIN Xiao,MO Jian-guang.Research and Development of Preparation High Performance Liquid Chromatography System for Isolation and Purification[J].Journal of Guangxi Academy of Sciences,2010,26(3):354-356. [点击复制]
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| 制备高效液相色谱分离纯化系统的研制与开发 |
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刘布鸣1, 马彦2, 冯可荣3, 黄艳1, 王廷伟2, 林霄1, 莫建光4
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| (1.广西中医药研究院, 广西南宁 530022;2.广西南宁市威玛龙色谱科技有限公司, 广西南宁 530022;3.广西计量检测研究院, 广西南宁 530022;4.广西分析测试研究中心, 广西南宁 530022) |
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| 摘要: |
| 介绍一种基于柱层析技术、高效液相色谱技术于一体的计算机智能控制全自动、高性能的化学物质纯化系统。该系统属于高压制备高效液相色谱,采用模块化设计模式,各模块经由计算机工作站软件统一协调,实现进样、分离、馏分收集自动化。该系统应用于中药复杂成分分离、提取和纯化的效率高、馏分损失少、样品回收率高。 |
| 关键词: 制备色谱系统 分离 纯化 工作站 |
| DOI： |
| 投稿时间：2010-06-05 |
| 基金项目:广西创新能力建设项目(09-090-10C)资助。 |
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| Research and Development of Preparation High Performance Liquid Chromatography System for Isolation and Purification |
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LIU Bu-ming1, MA Yan2, FENG Ke-rong3, HUANG Yan1, WANG Ting-wei2, LIN Xiao1, MO Jian-guang4
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| (1.Guangxi Institute of Traditional Medical and Pharmaceutical Science, Nanning, Guangxi, 530022, China;2.Guangxi Nanning Weimar Technology Co., Ltd. Dragon chromatography, Nanning, Guangxi, 530022, China;3.Guangxi Institute of Metrology and Test, Nanning, Guangxi, 530022, China;4.Guangxi Research Center of Analysis and Testing, Nanning, Guangxi, 530022, China) |
| Abstract: |
| A purification system based on column chromatography and high performance liquid chromatography with automated computer intelligent control was introduced.The system used high pressure for preparation high performance liquid chromatography and modular designed modes.All modes are coordinated by computer workstation software to implement sample injection, separation and fraction collection automatedly. The instrument can be used to separate, extract and purify complex components in traditional Chinese medicine with high efficiency of separation and purification, low loss fraction and high recovery rate. |
| Key words: preparation high performance liquid chromatography system isolation purification workstation |
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