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  • 桂柳成,邹华红,程蕾,胡坤.二氧化硅微球场发射环境扫描电镜形貌测试条件研究[J].广西科学院学报,2010,26(3):349-353.    [点击复制]
  • GUI Liu-cheng,ZOU Hua-hong,CHENG Lei,HU Kun.Research on Field Environmental Scanning Electron Microscope Observation Conditions of SiO2 Micro-ball[J].Journal of Guangxi Academy of Sciences,2010,26(3):349-353.   [点击复制]
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二氧化硅微球场发射环境扫描电镜形貌测试条件研究
桂柳成, 邹华红, 程蕾, 胡坤
0
(药用资源化学与药物分子工程教育部重点实验室, 广西师范大学化学化工学院, 广西桂林 541004)
摘要:
以二氧化硅微球作为研究对象,室温下采用场发射环境扫描电镜(FEI Quanta 200),选用二次电子(SE)成像进行SEM观察。分别考察镀膜处理、加速电压、束斑变化、扫描速度、工作距离等参数对图像质量的影响。
关键词:  图像质量  二氧化硅微球  镀膜  加速电压  束斑变化  扫描速度  工作距离
DOI:
投稿时间:2010-06-12
基金项目:
Research on Field Environmental Scanning Electron Microscope Observation Conditions of SiO2 Micro-ball
GUI Liu-cheng, ZOU Hua-hong, CHENG Lei, HU Kun
(Key Laboratory for the Chemistry and Molecular Engineering of Medicinal Resources(Ministry of Education of China), School of Chemistry & Chemical Engineering of Guangxi Normal University, Guilin, Guangxi, 541004, China)
Abstract:
SiO2 micro-ball was studied by Field Environmental Scanning Electron Microscope with secondary electron (SE) imaging at room temperature.Effect of different parameters including coating treatment,accelerating voltage,the spot changes,scanning speed,working distance,etc.,on image quality was investigated.
Key words:  image quality  SiO2 micro-ball  coating treatment  accelerating voltage  beam spot  scanning speed  working distance

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