| 引用本文： |
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雷富,许铭本,何小英,张荣灿,姜发军.角鲨烯软胶囊中角鲨烯的鉴定和分析[J].广西科学院学报,2011,27(3):199-201. [点击复制]
- LEI Fu,XU Ming-ben,He Xiao-ying,ZHANG Rong-can,JIANG Fa-jun.Identification and Analysis of Squalene in Capsule[J].Journal of Guangxi Academy of Sciences,2011,27(3):199-201. [点击复制]
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| 摘要: |
| 用红外光谱和质谱对角鲨烯软胶囊中的角鲨烯进行成分鉴定,用气相色谱-质谱法测定角鲨烯含量。结果表明:所建立的气相色谱-质谱定量分析方法的平均回收率为98.7%,相对标准偏差为5.9%,线性相关系数为0.9999,最低检出限为0.6ng/ml。 |
| 关键词: 角鲨烯 气相色谱-质谱 红外光谱 |
| DOI： |
| 投稿时间：2010-07-23 |
| 基金项目:广西科学院基本科研业务费项目(编号:09YJ17HY01)资助 |
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| Identification and Analysis of Squalene in Capsule |
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LEI Fu, XU Ming-ben, He Xiao-ying, ZHANG Rong-can, JIANG Fa-jun
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| (Guangxi Academy of Sciences, Nanning, Guangxi, 530007, China) |
| Abstract: |
| Infrared spectroscopy and mass spectrometry were used to identify squalene in capsule,and the content of squalene was analyzed by gas chromatography-mass spectrometry.Results showed that the average recovery of the quantitative analysis established by gas chromatography-mass spectrometry was 98.7%;the relative standard deviation was 5.9%;linear correlation coefficient was 0.9999;the detection limit was 0.6ng/ml. |
| Key words: squalene gas chromatography-mass spectrometry infrared |
