| 摘要: |
| 以对羟基苯甲酸和尿素为基本原料,在脱水剂和催化剂共同作用下,直接酰胺化一锅法合成对羟基苯甲腈,并采用熔点测定和红外分析方法判定产物结构。 |
| 关键词: 对羟基苯甲腈 酰胺反应 一锅法 |
| DOI： |
| 投稿时间：2010-06-28 |
| 基金项目: |
|
| Synthesis and IR Analysis of 4-Hydroxybenzonitrile |
|
GUO Yi-feng1, CHEN Ping1,2
|
| (1.Faculty of Material Science & Engineering, Guilin University of Technology, Guilin, Guangxi, 541004, China;2.Key Laboratory of New Processing Technology for Nonferrous Metals and Materials Constituted by Ministry of Education, Guilin University of Technology, Guilin, Guangxi, 541004, China) |
| Abstract: |
| 4-Hydroxybenzonitrile, which is one important fine chemical intermediates, was synthesized by 4-hydroxybenzonic acid and urea through acylating reaction and dehydrating reaction. The structure of 4-hydroxybenzonitrile was characterized by FT-IR and melt-point analysis. |
| Key words: 4-Hydroxybenzonitrile acylating reaction one-Pot Synthesis |
