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  • 谢文佩,林琳,龙彬,何碧娟,高程海.北部湾网状软柳珊瑚化学成分研究[J].广西科学,2013,20(2):165-167.    [点击复制]
  • XIE Wen-pei,LIN Lin,LONG Bin,HE Bi-juan,GAO Cheng-hai.Chemical Constituents from the Beibu Gulf gorgonian Suberogogorgia reticulat[J].Guangxi Sciences,2013,20(2):165-167.   [点击复制]
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北部湾网状软柳珊瑚化学成分研究
谢文佩1,2, 林琳1,2, 龙彬1,2, 何碧娟2, 高程海2
0
(1.广西大学轻工与食品工程学院, 广西南宁 530004;2.广西科学院, 广西南宁 530007)
摘要:
采用柱色谱、凝胶层析和高效液相色谱分离技术,从网状软柳珊瑚(Suberogogorgia reticulat)中分离获得8个单体化合物。运用理化和波谱分析,分别鉴定为cholest-5-en-3β-ol(1)、尼克酰胺(2)、咖啡碱(3)、腺嘌呤(4)、1,7,9-trimethyl-1H-purine-6,8(7H,9H)-dione(5)、尿嘧啶(6)、胸腺嘧啶(7)、对羟基苯甲酸(8)。化合物1,2,4,5,8均是首次从该种海洋动物中分离得到。
关键词:  网状软柳珊瑚  化合物  结构鉴定
DOI:
投稿时间:2012-11-28修订日期:2013-01-16
基金项目:国家自然科学基金项目(81260480),广西科技攻关项目(桂科攻1114011-7),广西自然科学基金项目(2011GXNSFB018035,2011GXNSFE018002,2012GXNSFAA053160,2012GXNSFEA053001)资助。
Chemical Constituents from the Beibu Gulf gorgonian Suberogogorgia reticulat
XIE Wen-pei1,2, LIN Lin1,2, LONG Bin1,2, HE Bi-juan2, GAO Cheng-hai2
(1.College of Light Industry and Food Engineering, Guangxi University, Nanning, Guangxi, 530004, China;2.Guangxi Academy of Sciences, Nanning, Guangxi, 530007, China)
Abstract:
Eight compounds (1~8) were isolated from the Beibu Gulf gorgonian Suberogogorgia reticulat.Their structures were identified as cholest-5-en-3β-ol (1),nicotinamide (2),caffeine (3),adenine (4),1,7,9-trimethyl-1H-purine-6,8(7H,9H)-dione (5),uracil (6),6-methyluracil (7),and 4-hydroxybenzoic acid (8) on the basis of extensive spectroscopic analysis.Compounds 1,2,4,5,and 8 were isolated from the invertebrate for the first time.
Key words:  Suberogogorgia reticulat  compounds  chemical identification

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