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  • 肖乃玉,李善吉.路易斯酸催化合成香料醋酸苯甲酯[J].广西科学,2010,17(2):135-137.    [点击复制]
  • XIAO Nai-yu,LI Shan-ji.Synthesis of Flavor Benzyl Acetate with Lewis Acid as a Catalyst[J].Guangxi Sciences,2010,17(2):135-137.   [点击复制]
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路易斯酸催化合成香料醋酸苯甲酯
肖乃玉1, 李善吉2
0
(1.仲恺农业工程学院轻工食品学院, 广东广州 510225;2.嘉应学院化学与环境学院, 广东梅州 514015)
摘要:
研究以路易斯酸氯化锌为催化剂,乙酸和苄醇为原料合成醋酸苯甲酯的工艺条件。结果表明,反应的最佳条件是:冰醋酸:苯甲醇=1.0:2.0,带水剂10ml,催化剂1.5g,回流反应时间2.5h。在此条件下,酯收率达到93.2%。
关键词:  路易斯酸  香料  醋酸苯甲酯
DOI:
投稿时间:2010-01-27修订日期:2010-04-06
基金项目:
Synthesis of Flavor Benzyl Acetate with Lewis Acid as a Catalyst
XIAO Nai-yu1, LI Shan-ji2
(1.School of Light Industry and Food Science, Zhongkai University of Agriculture and Engineering, Guangzhou, Guangdong, 510225, China;2.College of Chemistry and Environment, Jiaying University, Meizhou, Guangdong, 514015, China)
Abstract:
The technological conditions that benzyl acetate was synthesized from acetic acid and benzyl alcohol with Lewis acid zinc chloride as catalyst were studied, The results showed that the optimum reaction conditions were benzyl alcohol:acetic acid=2.0:1.0,the taking water reagent 10 ml, amount of catalyst 1.5g and yield of benzyl acetate could reach 93.2%.
Key words:  Lewis acid  flavor  benzyl acetate

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