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  • 高程海,龙彬,苏志维,余炼,颜栋美,文良娟,何碧娟.红树木榄胚轴中芳香环类化学成分研究[J].广西科学院学报,2015,31(1):28-31.    [点击复制]
  • GAO Cheng-hai,LONG Bin,SU Zhi-wei,YU Lian,YAN Dong-mei,WEN Liang-juan,HE Bi-juan.Study on Aromatic Compounds from Hypocotyls of Mangrove Bruguiera gymnorrhiza[J].Journal of Guangxi Academy of Sciences,2015,31(1):28-31.   [点击复制]
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红树木榄胚轴中芳香环类化学成分研究
高程海1, 龙彬1,2, 苏志维1, 余炼1,2, 颜栋美2, 文良娟2, 何碧娟1
0
(1.广西科学院广西近海海洋环境科学重点实验室, 广西南宁 530007;2.广西大学轻工与食品工程学院, 广西南宁 530004)
摘要:
[目的]通过多种现代分析手段,探究木榄(Bruguiera gymnorrhiza)胚轴中芳香环类化学成分。[方法]采用现代柱色谱、凝胶层析和高效液相色谱分离技术,对木榄胚轴中芳香环类化学成分进行研究,并运用波谱分析和文献对照方法鉴定其化学结构。[结果]从木榄胚轴中分离鉴定了7个芳香环类单体化合物,分别鉴定为邻苯二甲酸-二-2-乙基己酯(1)、邻苯二甲酸二丁酯(2)、methyl caffeate(3)、原儿茶酸甲酯(4)、异香兰酸(5)、4-羟基苯甲酸(6)、4-甲氧基苯乙酸(7)。[结论]化合物1~7均是首次从该种海洋植物中分离得到。
关键词:  木榄  胚轴  芳香环  结构鉴定
DOI:
投稿时间:2014-07-10
基金项目:广西自然科学基金面上项目(2014GXNSFAA118048,2012GXNSFAA053160),广西近海海洋环境科学重点实验室开放基金项目(GXKLHY13-06)和广西区科技攻关项目(桂科合14123001-7)资助。
Study on Aromatic Compounds from Hypocotyls of Mangrove Bruguiera gymnorrhiza
GAO Cheng-hai1, LONG Bin1,2, SU Zhi-wei1, YU Lian1,2, YAN Dong-mei2, WEN Liang-juan2, HE Bi-juan1
(1.Guangxi Key Laboratory of Marine Environmental Science, Guangxi Academy of Sciences, Nanning, Guangxi, 530007, China;2.College of Light Industry and Food Engineering, Guangxi University, Nanning, Guangxi, 530004, China)
Abstract:
[Objective] To investigate the aromatic compounds from the hypocotyls of mangrove Bruguiera gymnorrhiza by modern analysis methods.[Methods] Seven aromatic compounds were isolated and purified by repeated column chromatography on silica, sephadex LH-20 gel and HPLC. The structures of these compounds were identified by spectral analysis and literatures.[Results] Seven aromatic compounds were obtained from the hypocotyls of mangrove B.gymnorrhiza and characterized as Di-(2-ehtylhexyl) phthalate(1),Dibutyl phthdate (2),Methyl caffeate (3),(Z)-4-Coumaric acid 4-O-β-D-glucopyranoside (4),3-hydroxy-4-methoxybenzoic acid (5),4-hydroxybenzoic acid (6),4-methoxyphenylacetic acid (7).[Conclusion] Compounds 1~7 were isolated from this plant for the first time.
Key words:  Bruguiera gymnorrhiza  hypocotyl  aromatic compound  structure identification

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