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  • 姚彩璐,何锦锋,张枝芝.平板玻璃熔融包裹体的拉曼光谱分析研究[J].广西科学院学报,2014,30(3):208-210.    [点击复制]
  • YAO Cai-lu,HE Jin-feng,ZHANG Zhi-zhi.Analysis of Melt Inclusions Defects of Flat Glass by Raman Spectra[J].Journal of Guangxi Academy of Sciences,2014,30(3):208-210.   [点击复制]
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平板玻璃熔融包裹体的拉曼光谱分析研究
姚彩璐1, 何锦锋2, 张枝芝3,4
0
(1.南宁浮法玻璃有限责任公司, 广西南宁 530031;2.北海市产品质量检验所, 广西北海 536000;3.广西师范大学物理科学与技术学院, 广西桂林 541004;4.广西科学院生物物理与环境科学研究中心, 广西南宁 530007)
摘要:
[目的]玻璃生产过程中玻璃表面和内部经常会出现多种类型的熔融包裹体,了解包裹体的成分对分析其形成以及调整玻璃生产工艺解决质量问题至关重要,传统的分析方法在很多时候需要制片,而且需要很丰富的经验,分析过程复杂、时间长,为此提出一种新的分析方法。[方法]基于显微拉曼光谱分析玻璃表面和内部的熔融包裹体,利用特征光谱判别包裹体的物质成分。[结果]成功鉴别出玻璃原材料中的长石、白云石、硅砂以及芒硝成分的包裹体,并通过岩相分析得以证实。[结论]显微拉曼光谱技术可以作为平板玻璃生产过程中质量缺陷分析的有效手段。
关键词:  玻璃  包裹体  拉曼光谱
DOI:
投稿时间:2014-04-10
基金项目:广西自然科学基金项目(2012GXNSFFA060008),国家自然科学基金项目(60868002)资助。
Analysis of Melt Inclusions Defects of Flat Glass by Raman Spectra
YAO Cai-lu1, HE Jin-feng2, ZHANG Zhi-zhi3,4
(1.Nanning Float Glass Limited Company, Nanning, Guangxi, 530031, China;2.Beihai Product Quality Testing Institute, Beihai, Guangxi, 536000, China;3.College of Physics and Technology, Guangxi Normal University, Guilin, Guangxi, 541004, China;4.Institute of Biophysics and Environmental Science, Guangxi Academic of Science, Nanning, Guangxi, 530007, China)
Abstract:
[Objective] There are different kinds of melt inclusions in float glass production.It is very important to know the ingredients of melt inclusions and their formations in order to realignment process parameters for solving the quality problem.The lithofacies method is the traditional analytical method,but in many cases,this method needs to cut the glass into slices,which requires rich experience,along with complex and time consuming analysis process,so a new method is induced.[Methods] With micro Raman spectroscopy spectral glass surface and internal melt inclusions are analyzed using the characteristic spectrum to distinguish ingredients of the melt inclusions.[Results] This paper successfully using Raman spectroscopy analyzes the feldspar,dolomite,silica sand as well as the composition of glauber's salt inclusions from glass raw materials,with verification by petrographic analysis.[Conclusion] The results show that the micro Raman spectroscopy can be used as a useful tool for quality defects analysis in flat glass production process.
Key words:  glass  melt inclusion  raman spectrum

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