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  • 梁宇,马琛,龙凤,黄锁义.硫酸铁催化合成橙花素[J].广西科学院学报,2006,22(1):25-26.    [点击复制]
  • LIANG Yu,MA Chen,LONG Feng,HUANG Suo-yi.Catalytic Synthesis of β-Naphthol Ethylether with Ferric Sulfate[J].Journal of Guangxi Academy of Sciences,2006,22(1):25-26.   [点击复制]
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硫酸铁催化合成橙花素
梁宇, 马琛, 龙凤, 黄锁义
0
(右江民族医学院, 广西百色 533000)
摘要:
应用硫酸铁作催化剂,将β-萘酚与无水乙醇反应合成橙花素。最佳反应条件是:物质的量比为β-萘酚:无水乙醇:硫酸铁=1:5.48:0.05,产率为83.7%。该方法反应条件温和,操作方便,对环境污染小,收率高,是合成橙花素的好方法。
关键词:  橙花素  硫酸铁  β-萘酚  无水乙醇  催化  合成
DOI:
投稿时间:2005-03-30修订日期:2005-06-20
基金项目:
Catalytic Synthesis of β-Naphthol Ethylether with Ferric Sulfate
LIANG Yu, MA Chen, LONG Feng, HUANG Suo-yi
(Youjiang Medical College for Nationalities, Baise, Guangxi, 533000, China)
Abstract:
β-Naphthol ethylether was synthesized in the reaction of β-naphthol and ethyl alcohol in the catalysis of ferric sulfate.The optimum reaction conditions are released as follows.Molar ratio of β-naphthol to ethyl alcohol to ferric sulfate is 1:5.48:0.05.The production efficiency reaches 83.7%.This method is moderate in reaction,and is convenience in operation without pollution to environment.
Key words:  β-naphthol ethylether  ferric sulfate  β-naphthol  ethyl alcohol  catalysis  synthesis

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