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梁威,刘元,宋志钊,文志云.瑶药瑞香通养助孕胶囊质量控制研究[J].广西科学,2015,22(6):627-630. [点击复制]
- LIANG Wei,LIU Yuan,SONG Zhi-zhao,WEN Zhi-yun.Study on Quality Control Standards of Yao Medicine Ruixiangtongyangzhuyun Capsules[J].Guangxi Sciences,2015,22(6):627-630. [点击复制]
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| 瑶药瑞香通养助孕胶囊质量控制研究 |
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梁威1,2, 刘元1,2, 宋志钊1,2, 文志云1,2
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| (1.广西中医药研究院, 广西南宁 530022;2.广西中药质量标准研究重点实验室, 广西南宁 530022) |
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| 摘要: |
| [目的]建立瑶药瑞香通养助孕胶囊质量标准。[方法]采用TLC法对处方中毛瑞香和地榆进行定性鉴别,并采用HPLC法测定岩白菜素的含量。[结果]毛瑞香和地榆薄层色谱图斑点清晰,重现性好,无干扰;岩白菜素在10.5~168.0 μg·mL-1线性良好,r=0.9998,平均回收率为98.9%,RSD为1.23%(n=6)。[结论]建立的质量控制方法可有效控制瑶药瑞香通养助孕胶囊的质量。 |
| 关键词: 瑞香通养助孕胶囊 瑶药 TLC HPLC 岩白菜素 |
| DOI： |
| 投稿时间：2015-08-10修订日期：2015-10-20 |
| 基金项目:广西科技攻关项目(桂科攻1346008-7),广西卫生厅重点科研课题项目(重S201308-06)和广西瑶族习用药材质量评价与标准研究项目(MZY2012025)资助。 |
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| Study on Quality Control Standards of Yao Medicine Ruixiangtongyangzhuyun Capsules |
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LIANG Wei1,2, LIU Yuan1,2, SONG Zhi-zhao1,2, WEN Zhi-yun1,2
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| (1.Guangxi Institute for Chinese Medicine & Pharmaceutical Science, Nanning, Guangxi, 530022, China;2.Guangxi Key Laboratory of Traditional Chinese Medicine Quality Standards, Nanning, Guangxi, 530022, China) |
| Abstract: |
| [Objective] This study was conducted to set up the quality control standards of Yao medicine Ruixiangtongyangzhuyun capsules.[Methods] Daphnes atrocaulis Herbs and garden burnet were identified qualitatively by TLC methods, while bergenin content was determined by HPLC method.[Results] The TLC figures of the two extracts were distinct, reproducible and noninterference.The calibration curves were linear in the range of 10.5~168.0 μg·mL-1 for bergenin (r=0.9998), average recovery of bergenin was 98.9%.and RSD was 1.23%(n=6). [Conclusion] The quality of Yao medicine Ruixiangtongyangzhuyun capsule can be effectively controlled by these quality standards. |
| Key words: Ruixiangtongyangzhuyun capsules Yao medicine TLC HPLC bergenin |
