| 引用本文： |
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卢文杰,何开家,牙启康,陈家源,刘布鸣,谭晓,苏小川.长柱十大功劳石油醚部位的化学成分分析[J].广西科学,2009,16(1):79-81. [点击复制]
- LU Wen-jie,HE Kai-jia,YA Qi-kang,CHEN Jia-yuan,LIU Bu-ming,TAN Xiao,SU Xiao-chuan.Analysis of Chemical Constituents of Petroleum Ether Fraction from Mahonia duclouxiana Gagnep.[J].Guangxi Sciences,2009,16(1):79-81. [点击复制]
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| 摘要: |
| 通过硅胶柱层析从长柱十大功劳(Mahonia duclouxiana Gagnep.)药材的石油醚部位中分离得到5个油状流份,采用气相色谱-质谱-计算机联用技术(GC-MS-DS)分别对它们的化学成分进行分析和鉴定。结果检出50个成分,鉴定出其中41个成分,检出率为82%。所有化合物均为首次从该植物中分离鉴定。 |
| 关键词: 长柱十大功劳 油状流份 气相色谱-质谱联用 |
| DOI： |
| 投稿时间：2008-10-30修订日期：2008-12-16 |
| 基金项目:广西自然科学基金项目(桂科自0832226);广西大型仪器协作共用资金项目(685-2008-093)资助 |
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| Analysis of Chemical Constituents of Petroleum Ether Fraction from Mahonia duclouxiana Gagnep. |
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LU Wen-jie1, HE Kai-jia1, YA Qi-kang1, CHEN Jia-yuan1, LIU Bu-ming1, TAN Xiao1, SU Xiao-chuan2
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| (1.Guangxi Institute of Traditional Medical and Pharmaceutical Sciences, Nanning, Guangxi, 530022, China;2.Guangxi Center for Disease Prevention and Control, Nanning, Guangxi, 530022, China) |
| Abstract: |
| Five oil fractions of petroleum ether extract from Mahonia duclouxiana Gagnep.were isolated by silica gel column chromatography, and their chemical constituents were analyzed by GC-MS-DS technique, respectivily.As a result, 50 components were separated and 41 of them were identified.All the compounds were firstly identified from this plant. |
| Key words: Mahonia duclouxiana Gagnep. oil fraction GC-MS-DS |
