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  • 陈全斌,杨建香,程忠泉,义祥辉,韦正波.罗汉果叶黄酮甙的分离与结构鉴定[J].广西科学,2006,13(1):35-36,42.    [点击复制]
  • CHEN Quan-bin,YANG Jian-xiang,CHENG Zhong-quan,YI Xiang-hui,WEI Zheng-bo.Separation, Purification and Identification of Flavonol Glycoside from Momordica grosvenori Leafs[J].Guangxi Sciences,2006,13(1):35-36,42.   [点击复制]
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罗汉果叶黄酮甙的分离与结构鉴定
陈全斌1, 杨建香2, 程忠泉2, 义祥辉2, 韦正波3
0
(1.广西师范大学资源与环境学系, 广西桂林 541004;2.桂林师范高等专科学校, 广西桂林 541001;3.广西医科大学附属肿瘤医院, 广西南宁 530021)
摘要:
以罗汉果叶为原料提取黄酮,用溶剂萃取、柱层析、HPLC纯化等方法进行黄酮甙的分离和提纯后,采用TLC、HPLC、IR、NMR、MS等分析方法进行结构鉴定。结果表明,罗汉果叶含有2种黄酮甙,它们分别是:山奈酚-3,7-O-α-L-二鼠李糖甙和槲皮素-3-O-β-D-葡萄糖7-O-α-L-鼠李糖甙。
关键词:  罗汉果    黄酮甙  结构鉴定
DOI:
投稿时间:2005-07-05修订日期:2005-08-22
基金项目:广西科学研究与技术开发计划项目(桂科能0443001-12);广西师范大学重点科研项目(2005-2007)。
Separation, Purification and Identification of Flavonol Glycoside from Momordica grosvenori Leafs
CHEN Quan-bin1, YANG Jian-xiang2, CHENG Zhong-quan2, YI Xiang-hui2, WEI Zheng-bo3
(1.Department of Resources and Environment, Guangxi Normal University, Guilin, Guangxi, 541004, China;2.Guilin Normal College, Guilin, Guangxi, 541001, China;3.Tumor Hospital, Guangxi Medical University, Nanning, Guangxi, 530021, China)
Abstract:
The coarse flavone is extracted from Momordica grosvenori leaves by boiling water.Two compouns of flavone glycosides are obtained by silica gel column chromatography and HPLC purification.Two flavonol glycosides'structures are verified by different kinds of spectrum and chemistry methods.They are quercetin-3-O-β-D-glucose-7-O-α-L-rhamnopyranoside and kaempferol-3, 7-O-α-L-dirha-mnopyranoside.
Key words:  Momordica grosvenori  leaves  flavonol glycoside  structural identification

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