摘要: |
以十二水合硫酸铁铵为催化剂,采用单纯型搜索法优化柠檬酸三丁酯的合成工艺条件,产率达到97.18%。该工艺具有反应时间短,催化效率高,方法简单,不腐蚀,无污染等优点。 |
关键词: 柠檬酸三丁酯 单纯型搜索法 合成 |
DOI: |
投稿时间:2001-03-26 |
基金项目: |
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A New Synthesis Method of Tri(n-Butyl) Citrate |
Li Yuezhen, Li Fangliang
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(Department of Chemistry, Guangxi Nanning Prefecture Education College, Beihulu, Nanning, Guangxi, 530001, China) |
Abstract: |
Tri(n-butyl) citrate was synthesized with ammonium ferric sulfate dodecahydrate as catalyst,and the technological condition for the esterification systhesis was optimized by the simplex search method.The synthetic method has the advantages of high catalytic activity,easier operation,lower corrosion and no pollution. |
Key words: Tri (n-butyl) citrate simplex search method synthesis |