| 引用本文： |
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苏桂发,李新生,刘峥.微波辐射9,10-二氢蒽-9,10-桥-α,β-琥珀酰亚胺的N-烷基化反应研究[J].广西科学,2001,8(2):103-104. [点击复制]
- Su Guifa,Li Xinsheng,Liu Zheng.N-Alkylation of 9,10-Dihydroanthracene-9, 10-endo-α,β-succinimide under Microwave Irradiation Coupled with Phase Transfer Catalysis[J].Guangxi Sciences,2001,8(2):103-104. [点击复制]
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| 摘要: |
| 将微波辐射和相转移催化技术相结合,用于7个溴代烷(溴乙烷→溴辛烷)与9,10-二氢蒽-9,10-桥-α,β-琥珀酰亚胺的烷基化反应。反应时间快(1min~3min),产率高(88%~98%)、操作简便。 |
| 关键词: 微波辐射 相转移催化 9,10-二氢蒽-9,10-桥-α,β-琥珀酰亚胺 烷基化 |
| DOI： |
| 投稿时间：2001-01-16修订日期：2001-03-14 |
| 基金项目: |
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| N-Alkylation of 9,10-Dihydroanthracene-9, 10-endo-α,β-succinimide under Microwave Irradiation Coupled with Phase Transfer Catalysis |
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Su Guifa, Li Xinsheng, Liu Zheng
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| (Department of Chemistry and Chemical Engineering, Guangxi Normal University, 3 Yucailu, Guilin, Guangxi, 541004, China) |
| Abstract: |
| Microwave irradiation coupled with phase transfer catalysis was applied in the N-alkylation reaction of seven bromo-compounds(bromoethane to octyl bromide) with 9,10-dihydroanthracene-9 and 10-endo-α,β-succinimide.The reaction can complete in one to three minutes.The production rate is up to 88% to 98%, and operation is simple. |
| Key words: microwave irradiation phase transfer catalysis 9,10-dihydroanthracene-9,10-endo-α,β-succinimide alkylation |
